Labelled peptides

Details Labelled peptides Labelled peptides

1976-04-14

1977-08-09

Phillips, Delbert R.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

2603262, 2605342, C07C10352

Patent

active

040410234

ABSTRACT:
Radiolabelled and isotopically labelled peptides are prepared in a convenient and efficient manner by catalytically tritiating or deuterating an analog of the desired peptide containing one or more amino acid residues having an ethylenic type unsaturated bond therein. Preferred amino acid residues for this purpose include 3,4-dehydroproline (.DELTA..sup.3 -proline) and trans-4,5-dehydrolysine (.DELTA..sup.4 -lysine).

REFERENCES:
J. Am. Chem. Soc. 84, 1697-1701 (1962).
Biochem. & Biophysics 154, 483-87. (1973).

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