Kinetic assay for inorganic phosphates and composition therefore

Chemistry: molecular biology and microbiology – Measuring or testing process involving enzymes or... – Involving transferase

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G01N 3114, G01N 3316

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active

041599233

ABSTRACT:
A kinetic assay is provided for determining the inorganic phosphate content in an aqueous solution by measuring the amount of reduced coenzyme produced. The assay is based on the following coupled reactions:
I. maltose+PO.sub.4.sup.-3 maltose phosphorylase glucose+.beta.-D-glucose-1-phosphate;
Ii. .beta.-d-glucose-1-phosphate .beta.-D-phosphoglucomutase glucose-6-phosphate;
Iii. glucose-6-phosphate+NAD glucose-6-phosphate dehydrogenase NADH+6-phosphogluconate.

REFERENCES:
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patent: 4000042 (1976-12-01), Adams
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Bergmeyer, Methods of Enzymatic Analysis, vol. 1, Academic Press, New York, 1974, pp. 109-110 and 123-127.
Bergmeyer, Methods of Enzymatic Analysis, vol. 4, Academic Press, New York, 1974, pp. 2234-2238.
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Fitting et al., "Phosphorolysis of Maltose by Enzyme Preparations from Neiserra Meningitidis", J. Biol. Chem., vol. 199, pp. 153-163 (1952).
Ben-Zui et al., "A Phosphoglucomutase for Beta-glucose-1-phosphate", Biochem. Biophys. Res. Com. vol. 2, NO. 1, pp. 8-11 (1960).
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Ben-Zui et al., "A Phosphoglucomutase Specific for Beta-glucose-1-phosphate", J. Bio. Chem., vol. 236, pp. 2186-2189 (1961).

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