Jet mixing in preparation of monodisperse silver halide emulsion

Radiation imagery chemistry: process – composition – or product th – Radiation sensitive product – Silver compound sensitizer containing

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G03C 102

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active

042516277

ABSTRACT:
A process for preparing a photographic emulsion having a controlled grain size, structure, and size distribution, wherein a silver salt and an alkali metal halide react to precipitate silver halide grains at uniform pAg using high velocity mixing jets directed vertically downward to accomplish rapid dilution of and mixing of reactants in a conventional paddle-agitated precipitation vessel. A single recycle loop, or double recycle loops, feeds the mixing jets.

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patent: 3790386 (1974-02-01), Posse et al.
patent: 3821002 (1974-06-01), Culhane et al.
patent: 3897935 (1975-01-01), Forster
patent: 4147551 (1979-04-01), Finnicum et al.
Hautot, A. Photographic Theory 1962, pp. 17, 26, 27. Liege Summer School, 1962. The Focal Press. London and N. Y.
James, R. W. Photographic Emulsions-Recent Developments, 1973 pp. 131, 132; 1973; Noyes Data Corp. Ridgeway, N. J.

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