Isothermal calorimeter

Thermal measuring and testing – Calorimetry – Heat value of combustion

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Details

364557, G01K 1710, G01N 2516

Patent

active

053223608

ABSTRACT:
A calorimeter for determining the calorific value of a sample on the basis of the difference in temperature, measured on a real time basis, between the temperature of the water in a bucket containing the sample in a conventional calorimeter bomb and the temperature of the water in a reservoir maintained at substantially ambient temperature. The water from the reservoir is circulated by a pump through a heat exchanger, a water jacket surrounding the bucket and back to the reservoir in an effort to maintain the water in the system at ambient temperature. A method for calculating the corrected bucket temperature rise on the basis of Newton's Law of Cooling and for calculating the gross calorific value of the sample is also disclosed.

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"Precision Isoperibol Calorimeter with Automatic Data Acquisition and Processing," C. Shin et al., Review of Scientific Instruments, American Institute of Physics, vol. 46, No. 8, pp. 1043-1046, Aug. 1975.
"New Design of a Vacuum Jacket Precision Combustion Calorimeter," P. B. Arrken et al., The Review of Scientific Instruments, vol. 25, No. 10, Oct. 1954, pp. 967-970 (author unknown).
"Standard Test Method for Gross Calorific Value of Solid Fuel by the Isothermal Jacket Bomb Calorimeter," American National Standard ANSI/SSTM D3286-77, American Society for Testing & Materials, published Dec. 1977, pp. 1-10 (author unknown).
"Determination of the Gross Calorific Value of the Bomb Calorimeter and Calculation of the Net Calorific Value, Method Using Isothermal Water Jacket," DIN 51-900-German Standards (DIN-Normen), Aug. 1977, pp. 1-8 (author unknown).
"Heat of Combustion of Hydrocarbon Fuels by Bomb Calorimeter (High-Precision Method)," American Society for Testing & Materials, ANSI/ASTM D-2382-76, published Sep. 1976, pp. 1-12 (author unknown).

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