Organic compounds -- part of the class 532-570 series – Organic compounds – Oxygen containing
Patent
1994-09-01
2000-05-16
Kelly, C. H.
Organic compounds -- part of the class 532-570 series
Organic compounds
Oxygen containing
C07C 4100
Patent
active
060639660
ABSTRACT:
An impure methyl tertiary butyl ether product contaminated with isobutylene, methanol and water is purified by continuous counter-current contact with water and an isobutylene fraction in an extraction zone comprising a counter-current contact tower to provide an overhead raffinate comprising isobutylene, methyl tertiary butyl ether and a minor amount of water and an extract comprising methanol, water and a minor amount of methyl tertiary butyl ether; the overhead raffinate being separated in a methyl tertiary butyl ether purification distillation zone into a lighter distillation fraction comprising isobutylene and water and a heavier distillation fraction consisting essentially of methyl tertiary butyl ether; the lighter distillation fraction being decanted to remove water and to provide a distillate isobutylene fraction that is returned to the contact tower as the isobutylene fraction.
REFERENCES:
patent: 5243091 (1993-09-01), Kruse et al.
Peters Michael Warren
Sheu Yu-Hwa Edward
Brown Ron D.
Huntsman ICI Chemicals LLC
Kelly C. H.
Ries Carl G.
Stolle Russell R.
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