Intercalation of small graphite flakes with a metal halide

Details Intercalation of small graphite flakes with a metal halide Intercalation of small graphite flakes with a metal halide

1983-09-19

1986-08-05

Barr, Josephine L.

Chemistry of inorganic compounds

Carbon or compound thereof

Elemental carbon

423454, 423458, 252506, 252507, 252508, 556140, 523137, C01B 3102, H01B 106

Patent

active

046042768

ABSTRACT:
A method and apparatus for intercalating small graphite flakes with a metal halide. Graphite and a metal halide are placed in two chambers 12, 14 of a rotary vapor transport reactor assembly 10 and heated. The reactor is charged with a halogen gas and rotated by motor 24 during synthesis to produce a homogenous and uniform intercalated product.

REFERENCES:
patent: 3956194 (1976-05-01), Armand
patent: 4461719 (1984-07-01), Vogel et al.
"The Effect of Flake Size on Composition of Graphite Ferric Chloride", Hooley, J. A. & Somassy, R. N., Carbon, vol. 8, pp. 191-196.
"Intercalation Compounds of Graphite", Dresselhaus et al, Advances in Physics, vol. 30, No. 2, pp. 139-326 (1981).
"Graphite Intercalation Compounds", Fischer et al, Physics Today, pp. 36-45 (1978).
"Investigation into Methods for Producing Micron Particles from Graphite Flakes & Fibers", Tech. Proposal, GTE Labs. (8-82).

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