Instrument for the automated determination of organic halogens

Chemical apparatus and process disinfecting – deodorizing – preser – Analyzer – structured indicator – or manipulative laboratory... – Means for analyzing liquid or solid sample

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422 78, 422 57, 23230PC, G01N 3106, G01N 3112, G01N 3122

Patent

active

041608020

ABSTRACT:
A rapid, automated method for the determination of organic halogens is provided by an analytical system comprising a burner and combustion chamber for burning the organic halogen-containing sample in an oxygen-hydrogen flame; an absorption zone wherein the combustion gases are absorbed in a moving reagent film; and a colorimeter and recorder. With proper choice of reagent film, either total halogen (Cl, Br, I) content or specifically bromine content can be assayed automatically. The system is particularly useful for analysis of biological samples.

REFERENCES:
patent: 810870 (1906-01-01), Kirkwood
patent: 3141741 (1964-07-01), Hoel et al.
patent: 3298785 (1967-01-01), Ruel
patent: 4070155 (1978-01-01), Fraim
Automation in Analytical Chemistry, Technicon Symposia 1967, vol. I; Vernot et al., pp. 423-426.
White et al., A Method for the Rapid Determination of Trace Organic Halogens in Lipids Analytical Biochem, 78, 52-56 (1977).
Treatise on Analyt. Chem., Halogens Part II, vol. 7, pp. 353-391.

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