Inhibiting polymerization in extractive distillation of C-4 hydr

Distillation: processes – separatory – Addition of material to distilland to inhibit or prevent... – For inhibiting or preventing a polymerization reaction

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203 35, 203 51, 203 53, 203 57, 203 58, 203 60, 203 65, 585810, 585833, 585860, 585864, 585865, 585950, B01D 340, C07C 708

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042683610

ABSTRACT:
Formation of butadiene-1,3 polymer during the extractive distillation of a C-4 hydrocarbon mixture to separate and purify butadiene-1,3 using a solvent composition in which an alkoxynitrile is present in a proportion of 50-99 percent by weight, is decreased through inclusion in the solvent of a synergistic combination of 2,4-dinitrophenol and phosphoric acid, each in a proportion of 0.05 to 0.5 percent by weight.

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