Hydrothermal pretreatment to prevent scale during liquefaction o

Mineral oils: processes and products – Phenolic or toxic oils

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C10G 100

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044500661

ABSTRACT:
Scale formation during the liquefaction of lower ranking coals and similar carbonaceous materials is significantly reduced and/or prevented by hydrothermal pretreatment. The said pretreatment is believed to convert the scale-forming components to the corresponding carbonate prior to liquefaction. The said pretreatment is accomplished at a total pressure within the range from about 1000 to about 4400 psia. Temperature during said pretreatment will generally be within the range from about 500.degree. to about 700.degree. F.

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Chemical Rubber Co., Handbook 1971-1972 Ed. D-149.

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