Hydrothermal crystal growing apparatus

Chemical apparatus and process disinfecting – deodorizing – preser – Chemical reactor – Including means rotating reaction chamber during use

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422241, 422242, 422254, 156DIG98, C30B 710

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active

045592080

ABSTRACT:
Large single crystals of berlinite are grown onto seed crystals by maintaining the crystals at a fixed elevated temperature in a pressure vessel containing a nutrient of coarse berlinite crystalline powder, held at a fixed lower temperature, and concentrated phosphoric acid. Because berlinite shows retrograde solubility, the nutrient goes into solution, and berlinite deposits on the higher-temperature growing crystal. The vessel is rocked to promote motion of saturated solution to the crystal and depleted solution to the nutrient. Large single crystals of alpha-gallium orthophosphate may be grown using the same apparatus and a similar process. The resultant crystals may be cut into wafers useful in surface acoustic wave devices.

REFERENCES:
patent: 2675303 (1954-04-01), Sobek et al.
patent: 3271114 (1966-09-01), Kolb
patent: 3877875 (1975-04-01), Jones et al.
patent: 3920396 (1975-11-01), Schuy
patent: 4247358 (1981-01-01), Au Coin et al.
patent: 4324773 (1981-04-01), Chai et al.
patent: 4382840 (1983-05-01), Chai et al.
Hawley, Condensed Chemical Dictionary 8th Ed. 1971 p. 396.
Stanley, Industrial and Engineering Chemistry 8/54 vol. 46, No. 8, pp. 1684-1689.
Kolb et al., Jl. of Crystal Growth 43 (1978) pp. 313-319.
Webster, New World Dictionary, World Pub. Co. N.Y. 1968, College edition p. 109.

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