Hydrolysis of isocyanate distillation bottoms

Organic compounds -- part of the class 532-570 series – Organic compounds – Amino nitrogen containing

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564330, 564334, 564448, 564511, C07C 8750, C07C 8511, C07C 8714

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046544437

ABSTRACT:
Liquid distillation residue formed in the phosgenation of polyamines to form polyisocyanates are hydrolyzed to reform the polyamine. The process comprises forming an adduct of the distillation residue with additional polyamine and then hydrolyzing the resulting adduct to convert the adduct to said polyamine.

REFERENCES:
patent: 3225094 (1965-12-01), Wolf
patent: 3499035 (1970-03-01), Kober et al.

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