Hot melt method for preparing diphenhydramine tannate

Drug – bio-affecting and body treating compositions – Designated organic active ingredient containing – Peptide containing doai

Reexamination Certificate

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C536S119000

Reexamination Certificate

active

07001886

ABSTRACT:
The invention pertains to a method for preparing diphenhydramine tannate by reacting diphenhydramine free base at a temperature of about 75 to about 150° C. with tannic acid neat or as an aqueous slurry containing up to about 20 wt. % water. The diphenhydramine free base may be obtained by reacting a commercially available diphenhydramine salt such as diphenhydramine maleate with a base such as aqueous sodium hydroxide. The resultant diphenhydramine tannate has extended release properties and is useful in pharmaceutical compositions as an antihistamine for human beings.

REFERENCES:
patent: 5663415 (1997-09-01), Chopdekar et al.
patent: 6268012 (2001-07-01), Sikora et al.
patent: 6287597 (2001-09-01), Gordziel
patent: 6509492 (2003-01-01), Venkataraman

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