Highly compactable zirconium sponge and its manufacture

Specialized metallurgical processes – compositions for use therei – Processes – Producing or purifying free metal powder or producing or...

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241 23, B22F 900

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active

049254863

ABSTRACT:
The process for producing crushed zirconium sponge having particle configurations which enhance its compactability, wherein conventionally produced, as-reduced, non-sintered zirconium sponge pieces are loaded into a vacuum furnace, the furnace is heated under partial vacuum at a temperature of up to about 400.degree. C. for a sufficient period to essentially demoisturize and degas the sponge, the temperature is raised to at least about 700.degree. C. and the vacuum terminated, H.sub.2 is fed in a carefully controlled manner into the furnace over a period of several hours in a total amount comprising from about 0.05 to about 0.8% by weight of the sponge, the furnace is cooled, the cooled sponge is pacified, the sponge is removed from the furnace and crushed, the crushed sponge is loaded into a vacuum furnace, the furnace is heated at from about 950.degree. C. to about 1100.degree. C. under partial vacuum for a sufficient period to dehydride the sponge, and the dehydrided sponge, now of enhanced compactability, is cooled and recovered.

REFERENCES:
patent: 2829962 (1955-03-01), Supiro
patent: 4655825 (1987-04-01), Hard et al.

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