High temperature thermoelectric material and its production meth

Batteries: thermoelectric and photoelectric – Thermoelectric – Having particular thermoelectric composition

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136201, 1362361, 252 623T, 419 31, 419 38, 419 44, 419 53, 419 55, 419 56, 419 57, 420576, H01L 3518, H01L 3534, C22C 1200

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059124296

ABSTRACT:
Thermoelectric material for high temperature use made of a sintered body of a relative density of at least 75% consisting mainly of cobalt antimony compounds having an elemental ratio Sb/(Co+additives)=x of 2.7<x<3 is produced by a method of firing a shaped body of powders consisting mainly of cobalt and antimony in a non-oxidizing atmosphere under an environmental pressure, wherein the shaped body before the firing is constituted from crystal phases composed of a cubic crystal system compound CoSb.sub.3 (A phase), a monoclinic crystal system compound CoSb.sub.2 (B phase) and a hexagonal crystal system compound CoSb (C phase), and constitutional ratio of these crystal phases is (I.sub.B +I.sub.C)/(I.sub.A +I.sub.B +I.sub.C)<0.15 (wherein, I.sub.X (X is A, B or C) is a relative intensity by X-ray diffraction).

REFERENCES:
patent: 3454370 (1969-07-01), Castellion
patent: 3840652 (1974-10-01), Albers
patent: 5610366 (1997-03-01), Fleurial et al.
L.D. Dudkin and N.Kh. Abrikosov: "On the Doping of the Semiconductor Compound CoSb.sub.3 " pp. 126-133, Jan. 1958.
B.N. Zobrina and L.D. Dudkin: "Investigation of the Thermoelectric Properties of CoSb.sub.3 with Sn, Te and Ni Impurities" pp. 1668-1674, Dec., 1959.
K. Matsubara, T. Iyanaga, T. Tsubouchi, K. Kishimoto and T. Koyanagi: "Thermoelectric Properties of (pd, Co) Sb.sub.3 Compounds with Skutterudite Structure", 1995, pp. 226-229 Am. Inst. of Physics.
Thierry Caillat, Alex Borshchevsky and Jean-Pierre Fleurial: "Preparation and Thermoelectric Properties of p- and n-Type CoSb.sub.3 "; 1995 American Institute of Physics, pp. 58-61.
"Investigations of Several New Advanced Thermoelectric Materials at the Jet Propulsion Laboratory"; T. Caillat et al.; Proceedings Intersociety Energy Conversion Engineering Conference, Boston, 14th, 1979; Aug. 8, 1993 pp. 1.245-1.248, XP000428309 *p. 1245, paragraph 1*.

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