High surface area meixnerite from hydrotalcites

Chemistry of inorganic compounds – Oxygen or compound thereof – Metal containing

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C01F 716

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active

056458100

ABSTRACT:
A method for making a synthetic meixnerite which, when activated, has a high B.E.T. surface area, typically about 290 m.sup.2 /g or greater. The method comprises activating hydrotalcite, then cooling and hydrating such activated material in a carbon dioxide-free environment. Such hydration can produce a material that absorbs more than 100% of its weight in water. Following hydration, this material is activated a second time in a virtually carbon dioxide-free environment.

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Shen, J. et al, "Synthesis and Surface Acid/Base Properties of Magnesium-Aluminum Mixed Oxides Obtained from Hydrotalcites", Langmuir, vol. 10, No. 10, 1994, pp. 3902-3908.
Mascolo, G. et al, "A New Synthesis and Characterization of Magnesium-Aluminum Hydroxides", Mineralogical Magazine, Mar. 1980, vol. 43, pp. 619-621.
Pausch, I. et al, "Syntheses of Discordered and Al-Rich Hydrotalcite-Like Compounds", Clay and Clay Minerals, vol. 34, No. 5, 1986, pp. 507-510.
Dimotakis, E. et al, "Communications", Inorganic Chemistry, vol. 29, No. 13, Jun. 27, 1990, pp. 2393-2394.

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