High purity potassium tetrafluoroaluminate and method of making

Chemistry of inorganic compounds – Halogen or compound thereof – Plural metal or metal and ammonium containing

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423464, C01F 754

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active

052426696

ABSTRACT:
An improved method of making high quality potassium tetrafluoroaluminate. Hydrofluoric acid is added to high purity aluminum metal powder to form aluminum fluoride in solution. Nitric acid is added to this solution whereby impurities in the solution dissolve into the nitric acid. Water is then added to the solution to precipitate from the solution solid aluminum fluoride with impurities removed therefrom. The aluminum fluoride is then milled in the presence of hydrofluoric acid and potassium hydroxide whereby the exposure thereto produces the high quality potassium tetrafluoroaluminate which may then be washed and dried.

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