High pressure sample injection apparatus and method

Details High pressure sample injection apparatus and method High pressure sample injection apparatus and method

1974-08-01

1976-03-02

Swisher, S. Clement

Measuring and testing

Measuring vessel

G01N 110

Patent

active

039409945

ABSTRACT:
A high pressure sample injector for liquid chromatographs is disclosed. The apparatus includes structure defining a cylindrical dispensing chamber for receiving the sample to be injected into the flow path of a high pressure stream of carrier fluid in a liquid chromatograph. Control structure is interposed between the dispensing chamber and the flow path of the carrier stream for preventing liquid flow from the carrier stream to the dispensing chamber, and for enabling flow in the opposite direction only when the pressure in the dispensing chamber at least equals the carrier stream pressure. A pressurizing apparatus is connected to the dispensing chamber to raise its pressure, when desired, to a value at least equal to that of the carrier stream, in order that the sample may be injected into the carrier without reducing the carrier stream pressure.

REFERENCES:
patent: 3184973 (1965-05-01), Bradley
patent: 3186234 (1965-06-01), Solnick
patent: 3501176 (1970-03-01), Arms
Abel, Kenneth, Gas Sampling Valve for Closed System Sampling, Analytical Chemistry, Vol. 38, No. 6, May, 1966, pp. 806-807.

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