Heterocyclic-esters or -amides used as 5-HT.sub.4 receptor antag

Organic compounds -- part of the class 532-570 series – Organic compounds – Heterocyclic carbon compounds containing a hetero ring...

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546168, 546169, 546166, 546170, 546138, 514312, 514306, 514211, 514311, 514314, 540593, C07D215227, C07D21506, A61K 3147

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active

057081743

DESCRIPTION:

BRIEF SUMMARY
This invention relates to novel compounds having pharmacological activity, to a process for their preparation and to their use as pharmaceuticals.
European Journal of Pharmacology 146 (1988), 187-188, and Naunyn-Schmiedeberg's Arch. Pharmacol. (1989) 340:403-410, describe a non classical 5-hydroxytryptamine receptor, now designated the 5-HT.sub.4 receptor, and that ICS 205-930, which is also a 5-HT.sub.3 receptor antagonist, acts as an antagonist at this receptor. WO 91/16045 (SmithKline and French Laboratories Limited) describes the use of cardiac 5-HT.sub.4 receptor antagonists in the treatment of atrial arrhythmias and stroke.
EP-A-501322 (Glaxo Group Limited) describes indole derivatives having 5-HT.sub.4 antagonist activity.
WO 93/02677, WO 93/03725, WO 93/05038, WO 93/05040 and PCT/GB93/00506 (SmithKline Beecham plc) describe compounds having 5-HT.sub.4 receptor antagonist activity.
It has now been discovered that certain novel compounds also have 5-HT.sub.4 receptor antagonist properties.
When used herein, `treatment` includes prophylaxis as appropriate.
Accordingly, the present invention provides compounds of formula (I), wherein formula (I) consists of formulae (I-1) to (I-4), and pharmaceutically acceptable salts thereof, and the use of a compound of formula (I) or a pharmaceutically acceptable salt thereof: ##STR1## wherein X is O or S; CH(OR.sub.x)--(CH.sub.2).sub.2 wherein R.sub.x is hydrogen or C.sub.1-6 alkyl; alkoxy; or C.sub.1-6 alkylthio; ##STR2## wherein X is --N.dbd.CH--CH.dbd.CH-- or --NR.sub.4 --(CH.sub.2).sub.3 --; alkoxy; or C.sub.1-6 alkylthio; ##STR3## wherein X is O or NR.sub.4, where R.sub.4 is hydrogen or C.sub.1-6 alkyl; alkoxy; or C.sub.1-6 alkylthio; ##STR4## wherein X is --NR.sub.4 --CH.sub.2 CH--CH--; alkoxy; or C.sub.1-6 alkylthio; ##STR5## wherein n.sup.1 is 0, 1, 2, 3 or 4; n.sup.2 is 0, 1, 2, 3 or 4; n.sup.3 is 2, 3, 4 or 5; (CH.sub.2).sub.z --R.sub.10 wherein z is 2 or 3 and R.sub.10 is selected from cyano, hydroxyl, C.sub.1-6 alkoxy, phenoxy, C(O)C.sub.1-6 alkyl, COC.sub.6 H.sub.5, --CONR.sub.11 R.sub.12, NR.sub.11 COR.sub.12, SO.sub.2 NR.sub.11 R.sub.12 or NR.sub.11 SO.sub.2 R.sub.12 wherein R.sub.11 and R.sub.12 are hydrogen or C.sub.1-6 alkyl; and and heterocyclic bioisostere; activity.
Examples of alkyl or alkyl containing groups include C.sub.1, C.sub.2, C.sub.3, C.sub.4, C.sub.5, C.sub.6, C.sub.7, C.sub.8, C.sub.9, C.sub.10, C.sub.11 or C.sub.12 branched, straight chained or cyclic alkyl, as appropriate. C.sub.1-4 alkyl groups include methyl, ethyl, n- and iso-propyl, n-, iso-, sec- and tert-butyl. Cyclic alkyl includes cyclopropyl, cyclobutyl, cyclopentyl, cyclohexyl, cycloheptyl and cyclooctyl.
Aryl includes phenyl and naphthyl optionally substituted by one or more substituents selected from halo, C.sub.1-6 alkyl and C.sub.1-6 alkoxy.
Halo includes fluoro, chloro, bromo and iodo.
A suitable bioisostere for the amide or ester linkage containing Y in formula (I), is of formula (d): ##STR6## wherein the dotted circle represents one or two double bonds in any position in the 5-membered ring; H, J and I independently represent oxygen, sulphur, nitrogen or carbon, provided that at least one of H, J and I is other than carbon; U represents nitrogen or carbon.
Suitable examples of (d) are as described for X, Y and Z in EP-A-328200 (Merck Sharp & Dohme Ltd.), such as an oxadiazole moiety.
Y is preferably O or NH.
When Z is of sub-formula (a), n.sup.1 is preferably 2, 3 or 4 when the azacycle is attached at the nitrogen atom and n.sup.1 is preferably 1 when the azacycle is attached at a carbon atom, such as the 4-position when q is 2.
When Z is of sub-formula (b), n.sup.2 is preferably such that the number of carbon atoms between the ester or amide linkage is from 2 to 4 carbon atoms.
Suitable values for p and m include p=m=1; p=0, m=1, p=1, m=2, p=2, m=1.
When Z is of sub-formula (c), n.sup.3 is preferably 2, 3 or 4.
R.sub.8 and R.sub.9 are preferably both alkyl, especially one of R.sub.8 and R.sub.9 is C.sub.4 or larger alkyl.
Specific values of Z of particular inter

REFERENCES:
patent: 5620992 (1997-04-01), King
King, F.D. and Sanger, G.J; "5-HT.sub.3 Receptor Antagonists"; Drugs of the Future vol. 14, No. 9, 1989; pp. 875-889.
Evans S.M., Galdes, A., Gall, M.; "Molecular Modeling of 5-HT.sub.3 Receptor Ligands"; Pharmacology Biochemistry & Behavior, vol. 40, 1991; pp. 1033-1040.

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