Grinding amorphous silicon nitride powder prior to heating to pr

Chemistry of inorganic compounds – Silicon or compound thereof – Binary compound

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501 97, C01B 21068, C04B 3558

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active

045171688

ABSTRACT:
Crystalline silicon nitride powder in the form of granular particles having a large tap density and having good filling characteristics is produced by heating amorphous silicon nitride powder under an inert or reducing gas atmosphere. The amorphous silicon nitride powder is ground prior to the heating and the powder to be heated is maintained at a temperature of 1250.degree. C. to 1430.degree. C. for at least one hour in the course of temperature rise.

REFERENCES:
patent: 4073845 (1978-02-01), Buljan et al.
patent: 4196178 (1980-04-01), Iwai et al.
patent: 4208215 (1980-06-01), Kleiner et al.
patent: 4376652 (1983-03-01), Buljan
patent: 4405589 (1983-09-01), Iwai et al.

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