Graphite tube furnace with stationary specimen support for atomi

Optics: measuring and testing – By dispersed light spectroscopy – With sample excitation

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G01N 2174

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050838644

ABSTRACT:
A graphite tube furnace for atomic absorption spectroscopy has a specimen support. The graphite tube furnace is constructed with zones disposed substantially symmetrically around the center of the furnace. The shape of the zones is largely matched and matchable to the functions of the device, such as electric contacting, prevention of heat sinks, restriction of an atomization chamber, provision of an atomization chamber and holding of the specimen support. The specimen support is formed in such a way that in practice it is no longer heated by Joulean heat or thermal conduction, it is secured against movements and it has a minimal mass.

REFERENCES:
patent: 4303339 (1981-01-01), Glaser
patent: 4946278 (1990-08-01), Hutsch et al.
patent: 4971438 (1990-11-01), Hutsch et al.
Journal of Analytical Atomic Spectrometry, Mar. 1987, vol. 2, Ian L. Shuttler and H. Trevor Delves: "Between-Batch Variability of Thermal Characteristics of Commercially Available L'vov Platform Graphite Tube Atomisers, etc.", p. 171.
Lectures; Heinz Falk and Andreas Glismann: "Spatially and temporally resolved temperature profiles in graphite furnaces"; pp. 748 to 753, 1986, Fresenius Z Anal. Chem.

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