Graphite chuck having a hydrogen impervious outer coating layer

Chemistry of inorganic compounds – Silicon or compound thereof – Elemental silicon

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423348, C01B 3303

Patent

active

052846407

ABSTRACT:
The present invention is directed to a method for making substantially carbon-free polycrystalline silicon which comprises pyrolyzing a gaseous silicon compound on a heated starter filament mounted on a graphite chuck, said heated starter filament being maintained at a temperature sufficient to effect decomposition of the gaseous silicon compound to form polycrystalline silicon which is deposited thereon and by-product hydrogen, wherein the said graphite chuck is provided with a hydrogen impervious outer coating layer to prevent the by-product hydrogen from reacting with the graphite and form methane which decomposes as carbon on the deposited polycrystalline silicon.

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Wijaranakula et al., J. Electrochem. Soc., vol. 138, No. 7, Jul. 1991, pp. 2153-2159.
Sun et al., J. Appl. Phys. 67(9), 1 May 1990 pp. 4313-4319.
"CVD Coating for Industry and Aerospace" by Midland Materials Research, Inc., promotional literature (date unknown).

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