Coating processes – Particles – flakes – or granules coated or encapsulated – Solid encapsulation process utilizing an emulsion or...
Patent
1976-10-26
1978-10-03
Smith, Ronald H.
Coating processes
Particles, flakes, or granules coated or encapsulated
Solid encapsulation process utilizing an emulsion or...
427215, 252187H, C01B 1106
Patent
active
041185242
ABSTRACT:
Granular calcium hypochlorite particles having a core of calcium hypochlorite encapsulated in a plurality of layers of calcium hypochlorite are produced from an aqueous slurry of calcium hypochlorite by spraying a pumpable and sprayable slurry of calcium hypochlorite particles onto suspended particles of solid calcium hypochlorite above a moving bed of said particles. The solid particles coated with the slurry are heated to simultaneously evaporate and remove water from the slurry whereby said particles are coated with a layer of solid calcium hypochlorite.
A portion of the moving bed of coated articles is removed from the spraying zone and further processed, if desired. In one embodiment the coated articles, with or without sizing, are dried to produce granular particles having the desired moisture content. In another embodiment, the withdrawn portion is conveyed to another spraying zone where the articles are coated wth a slurry of calcium hypochlorite having a lower available chlorine content than the particles which form the core material. In another embodiment, the withdrawn portion of calcium hypochlorite particles is conveyed to another spraying zone where the particles are coated with a plurality of layers of an inorganic salt.
The resulting coated or layered granular particles of calcium hypochlorite have a high level of integrity and resist degradation and dusting when subjected to rather severe handling conditions. In addition, the novel granular calcium hypochlorite particles of this invention are highly stable when contacted wth lighted cigarettes, organic materials and the like.
REFERENCES:
patent: 2195756 (1940-04-01), Taylor
patent: 3761549 (1973-09-01), Marshall
patent: 3844726 (1974-10-01), Denaeyer
patent: 3953354 (1976-04-01), Faust
patent: 3969546 (1976-07-01), Saeman
Clements Donald F.
Haglind James B.
Olin Corporation
Silverberg Sam
Smith Ronald H.
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