Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal
Patent
1976-02-19
1978-04-04
Milestone, Norma S.
Chemistry of carbon compounds
Miscellaneous organic carbon compounds
C-metal
26034837, C07D30114
Patent
active
040827771
ABSTRACT:
This application discloses a process for manufacturing glycidol and, if desired, glycerol, by epoxidizing allyl alcohol with a 5 to 40% solution of peracetic acid in a substantially anhydrous, inert, organic solvent to produce glycidol in high yield and purity. Formation of by-products is minimized by rapid removal of co-product acetic acid. The glycidol can then be hydrolyzed to form a readily purifiable glycerol.
REFERENCES:
patent: 2977374 (1961-03-01), Phillips et al.
patent: 3374153 (1968-03-01), Naglieri
patent: 3625981 (1971-12-01), Kollar
Fisher Warren C.
Liao Hsiang-Peng
Linder Seymour M.
Pelley Ralph L.
FMC Corporation
Milestone Norma S.
Seems Eugene G.
Sheffer Abner
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