Glycidol and glycerol process

Details Glycidol and glycerol process Glycidol and glycerol process

1970-05-22

1976-05-04

Milestone, Norman S.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07D30114

Patent

active

039548155

ABSTRACT:
This application discloses a process for manufacturing glycidol, and, if desired, glycerol, by epoxidizing allyl alcohol with a 5 to 40% solution of peracetic acid in a substantially anhydrous, inert, organic solvent to produce glycidol in high yield and purity. Formation of by-products is minimized by rapid removal of co-product acetic acid. The glycidol can then be hydrolyzed to form a readily purifiable glycerol.

REFERENCES:
patent: 2977374 (1961-03-01), Phillips et al.

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