Gas chromatograph, Fourier transform, infrared spectroscopy syst

Measuring and testing – Gas analysis – Gas chromatography

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250343, 356410, G01N 2101, G01N 3108

Patent

active

044400136

ABSTRACT:
A gas chromatograph Fourier transform infrared (GC/FTIR) system includes a GC oven having a flexible capillary column therein for separating components of a sample. The column discharges effluent directly into a light pipe associated with an FTIR spectroscope. An auxiliary flow of carrier gas is added to the effluent at the light pipe to convey constituents through the light pipe free from tailing or peak broadening.

REFERENCES:
patent: 3444722 (1969-05-01), Roof
patent: 3649829 (1972-03-01), Randolf
patent: 3879984 (1975-04-01), Welland
patent: 3920334 (1975-11-01), Steichen et al.
patent: 4029416 (1977-06-01), Hawes
Brown et al., "Rapid Scan Infrared Spectrometer for Operation with Support Coated Tubular or Packed Column Gas Chromatographs", Anal. Chem., 42 (Mar. 1971), pp. 355-358.
Crawford et al., "Organic Analysis with a Combined Capillary GS/MS/FTIS", Anal. Chem. 54 (Apr. 1982), pp. 817-820.
Azarraga, "Gold Coating of Glass Tubes for GC/FTIRS, Light-Pipe Gas Cells", 34 (Mar. 1980), pp. 224-225.
M. D. Erickson, "Gas Chromatography/Fourier Transform Infrared Spectroscopy Applications", App. Spectrosc. Rev. 1979, 15, 261-325.

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