Formation of analyzable boron containing adducts

Details Formation of analyzable boron containing adducts Formation of analyzable boron containing adducts

1986-02-03

1987-12-15

Richman, Barry S.

Chemistry: analytical and immunological testing

Peptide, protein or amino acid

436 89, 436 90, 436 92, 436 93, 436 98, 436111, 436128, 436129, 436131, 436161, 436162, 436164, 436173, 436182, G01N 2400, G01N 3000, G01N 3300

Patent

active

047133465

ABSTRACT:
A method of forming analyzable adducts in a mixture of compounds by contacting the mixture with a boron reagent having the formula of either ##STR1## where each X and Y is, independently, an alkyl group of 12 or fewer carbons or an aryl group of 6-20 carbons; or BZ.sub.3, where each Z is, independently, an alkyl group of 12 or fewer carbons, or an aryl group of 6-20 carbons.

REFERENCES:
Megges et al, Chemical Abstracts, vol. 89, Abstract No. 159644x, 1978.
Gordon, Journal of the A.O.A.C., vol. 45, No. 3, pp. 785-786, 1962.
Nefkens et al., (1983), Tetrahedron 39:2295.
Fluckiger et al., (1984), Biomedical Mass Spectrometry 11:611.

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