Measuring and testing – Specimen stress or strain – or testing by stress or strain... – Indicating coating or sheet providing direct visual indication
Reexamination Certificate
2001-08-24
2002-10-08
Noori, Max (Department: 2855)
Measuring and testing
Specimen stress or strain, or testing by stress or strain...
Indicating coating or sheet providing direct visual indication
C073S800000
Reexamination Certificate
active
06460417
ABSTRACT:
BACKGROUND OF THE INVENTION
This invention relates to a method for determining mechanical properties of coating arrays. More particularly, the invention allows for the characterization of elongation and cracking of small-size coatings arranged in an array format.
Elongation properties of a coating material are of importance for automotive, telecommunication, and other applications. Conventional methods of elongation measurements involve the use of a large size coating material of about 100 mm in width and 150 mm in length, application of a conical mandrel test apparatus followed by a visual inspection of crack formation and measurement of the distance from the farthest end of the crack to the small end of the mandrel. The disadvantages of this standard method are the need to use a large coating area to obtain measurable parameters, manual measurements, difficulties in evaluation of several coatings simultaneously, and low sensitivity of measurements. A variety of test methods for elongation have been reported. These include the use of a CCD camera to measure the distance between the grid lines and calculate the elongation, automatic tensile test devices, devices to measure elongation due to bending under load, the use of lasers for noncontact elongation measurements and for the enlargement of the measuring range of speckle measuring systems of elongation.
Unfortunately, these techniques do not provide the capabilities for measurements of a large number of small-size coatings. What is needed are devices and methods for determining a variety of mechanical properties of multiple coating arrays. Such applications are of interest in combinatorial development of coating formulations and coatings.
SUMMARY OF THE INVENTION
The present invention solves the above-described problems by providing methods for testing elongation and cracking of coating arrays. In one embodiment, the method comprises simultaneously applying an elongating force to each of a plurality of coatings, and monitoring for a decrease in coating thickness and/or for cracks in each of the coatings. A relative performance characteristic of each coating is then determined based on a correlation between a measured decrease in coating thickness and/or a detected crack and the corresponding force.
In another embodiment, the method comprises depositing a plurality of coatings onto at least one substrate. The coatings are secured in a test arrangement, and a force is applied to each coating in order to bend the coatings. A detection system is then used to visualize cracks in the coatings and/or any decrease in coating thickness.
In still another embodiment of the present invention, the method comprises depositing a plurality of coatings onto at least one substrate, and securing the coatings in a test arrangement. A grid with a suitable scale is then applied onto each coating. A force is applied to each coating in order to bend the coating, and a detection system is used to visualize cracks in each coating and/or a decrease in coating thickness.
REFERENCES:
patent: 4031746 (1977-06-01), Kuruta et al.
patent: 4241801 (1980-12-01), Kushmuk
patent: 5193398 (1993-03-01), Harder et al.
patent: 5568259 (1996-10-01), Kamegawa
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patent: 6151123 (2000-11-01), Nielsen
patent: 6207030 (2001-03-01), Zdunek et al.
ASTM D 522-93a, Standard Test Methods for Mandarel Bend Test of Attached Organic Coatings; ASTM: 1993.
Cawse James Norman
Chisholm Bret Ja
Laurin Michael Matthew
Medford George Frederic
Olson Daniel Robert
Cabou Christian G.
General Electric Company
Johnson Noreen C.
Noori Max
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