Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – Cellular products or processes of preparing a cellular...
Patent
1985-11-19
1986-07-08
Foelak, Morton
Synthetic resins or natural rubbers -- part of the class 520 ser
Synthetic resins
Cellular products or processes of preparing a cellular...
521180, 521183, 521184, 521185, 521189, 528184, 528322, 528323, 528328, C08J 922, C08J 924
Patent
active
045993653
ABSTRACT:
Methods of foaming and fully curing polyimide resins entirely by the application of microwave energy. Foamable polyimide resins may be prepared by esterifying a suitable dianhydride, reacting the product with a suitable diamine, drying the resulting product and heating to spontaneously form a foam. In the past, such materials could be foamed but could not be satisfactorily cured to a resilient foam entirely by microwave energy. Post-foaming direct application of thermal energy was required to produce a satisfactory foam. We have found that adding a suitable oxoimine, such as caprolactam, to the reaction mixture results in a foam material which is fully and completely cured entirely by the application of microwave energy, considerably simplifying the process and reducing costs.
REFERENCES:
patent: Re31756 (1984-12-01), Gagliani et al.
Gagliani John
Long John V.
Foelak Morton
Gilliam Frank D.
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