Gas separation: processes – Liquid contacting – And recycle or reuse of contact liquid for further contact
Reexamination Certificate
1999-12-29
2001-04-24
Smith, Duane (Department: 1724)
Gas separation: processes
Liquid contacting
And recycle or reuse of contact liquid for further contact
C095S211000, C095S219000, C095S221000, C095S223000, C261S079200, C261S114300
Reexamination Certificate
active
06221133
ABSTRACT:
BACKGROUND OF THE INVENTION
This invention relates to packing elements for use in chemical process equipment. It relates specifically to packing elements of a novel and advantageous design that are particularly useful in separating vapors from entrained liquids while permitting counterflow contact to maximize mass transfer between the vapor and the liquid.
In distillation or fractionation towers in which a liquid and a vapor are contacted in a countercurrent flow to effect mass transfer, the vapor and liquid to some extent travel co-currently as a result of entrainment of the liquid in the vapor. There is a need to separate these components at the end of the passage through the tower to maintain efficient operation. The vapor entrains significant amounts of liquid during its passage, particularly if the vapor moves with a relatively high velocity. Separation of the entrained liquid is very desirable to complete the process and therefore various devices have been designed to accomplish this end.
While effective separation can be achieved by slowing the rate of flow, this is often impractical for reasons of space or efficiency of recycling. It is therefore highly desirable that the separation process be achieved “in-line”.
A particularly effective device is described in U.S. Pat. No. 5,683,493 which provides a plurality of packing elements or cells in vertically stacked layers. In each cell an upflowing vapor/liquid mixture enters through slits in the bottom and exits at the top into a cell in the layer above through slits in the bottom of that cell. Thus vapor/liquid mixture enters through slits in the bottom of a first cell and is caused to take on a rotational motion as it rises within the cell. This causes the liquid component to be expelled through slits in the outer wall of the cell into a downcomer connected to second similar cell offset below the first cell in which it meets an upflowing vapor/liquid mixture. Meanwhile the upflowing vapor from the first cell enters through slits in the bottom of a third cell located above the first cell. By having cells in adjacent layers off-set, the flows are caused to mix thus minimizing localized variations. This arrangement however carries with it certain space penalties that are preferably avoided. The present invention provides a packing system with liquid/vapor separation capabilities that comprises a series of identical cells stacked one on top of another which provide a highly compact and yet efficient structure for achieving the separation.
GENERAL DESCRIPTION OF THE INVENTION
The present invention provided a packing with vapor/liquid separation capabilities which comprises a cylindrical cell with a vertical axis having lower and upper portions and a chimney portion within the cylindrical cell wherein:
a) the lower portion has an annular base area with slots of a size to permit access of upflowing vapors when in use, surrounding an axially central cylinder of smaller cross-section which is open at the lower end and closed at the upper end and which communicates through radial slots adjacent the closed upper end with hollow static radial vanes which are angled with respect to the vertical and extend from the axially central cylinder and through the wall of the cylindrical cell into an annular jacket zone surrounding the cylindrical cell at a point adjacent the lower end of said jacket zone, said jacket zone being defined by the wall of the cylindrical cell and an outer co-axial jacket wall;
b) the upper portion is open and terminates at a point lower than the outer wall of the outer co-axial jacket zone and is provided with slots in the wall of the cylindrical cell; and
c) the chimney portion is coaxial with the cylindrical cell, has essentially the same length, has a diameter greater than the axially central cylinder and is provided with perforations adjacent to the lower end of the chimney portion allowing communication between the interior of the central chimney portion and the annular base area of the cylindrical cell.
The various components of the cell are described as being cylindrical but it should be understood that the term “cylindrical” is not limited to right cylinders but is intended to embrace cylinders with cross-sections that are polygonal or oval also. Generally however where the packing comprises a single stack of such cells, it is preferred that the jacket zone, the cylindrical cell, the central chimney portion and the axially central cylinder are co-axial and have cross-sections of the same shape but of course different dimensions.
In use a plurality of such cells are stacked vertically such that a vapor/liquid mixture enters through the slots in the base of a first cylindrical cell and comes into contact with the hollow angled static radial vanes which impart a radial motion to the flow as it rises within the cell. The heavier liquid is directed towards the wall of the cell and passes through the slots in the upper portion of the wall of the cell into the jacket zone. From the jacket zone the liquid exits through the hollow angled static radial vanes from which it flows into the axially central cylinder.
A second cell located below the first cell fits such that the upper end of the outer wall of the jacket zone of the second cell is in contact with the lower end of the outer wall of the jacket of the first cell.
Liquid flowing out through the passages in the axially central cylinder of the first cell enters the chimney portion of the second cell from which it flows through passages in the lower part of the chimney portion and over the slots in the base of the second cell through which vapor is rising.
Meanwhile vapor passing up through the first cell passes through slots in the base of a third cell located above the first cell.
The hollow static radial vanes can have any shape that achieves the directing effect such as rectangular or curved. Preferably however they have an aerofoil cross-section with a convex upper surface such that a vapor/liquid mixture passing over the vanes forms vortices that enhance the imparted radial motion promoting ejection of the liquid through the slots in the cell wall. The vanes also preferably have a direction that is also angled with respect to the radial direction established by the axis and the end of the vane closest to the axis so as to enhance the generation of a swirling motion within the cell.
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patent: 3817501 (1974-06-01), Tjutjunnikov et al.
patent: 4036917 (1977-07-01), Slobodyanik
patent: 4755198 (1988-07-01), Parton
patent: 5098615 (1992-03-01), Resetarits
patent: 5637263 (1997-06-01), Lang et al.
patent: 5660616 (1997-08-01), Choi et al.
patent: 5683493 (1997-11-01), Stober
patent: 5772870 (1998-06-01), Basse
patent: 5972171 (1999-10-01), Ross et al.
Bennett David
Norton Chemical Process Products Corporation
Pham Minh-Chau T.
Smith Duane
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