Flow-through shear analyzer for biologically active...

Chemical apparatus and process disinfecting – deodorizing – preser – Analyzer – structured indicator – or manipulative laboratory... – Means for analyzing liquid or solid sample

Reexamination Certificate

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C422S050000, C422S051000, C422S068100, C422S081000, C422S082000, C422S082070, C422S082080, C436S008000, C436S043000, C436S052000, C436S053000, C436S063000, C436S070000, C436S164000, C073S001010, C073S001020, C073S053010, C073S053040, C073S053060, C073S054020

Reexamination Certificate

active

06843963

ABSTRACT:
The adsorption rate of proteins from solutions on surfaces in the region of interface layers is often so large that a depletion of the protein in the interface layer results. Due to this, the total reaction becomes transport-dependent, sensitively disrupting the determination of the rate constants. In known TIRF-analysis chambers or bio-sensor systems with a liquid interface layer of ˜10 μm thickness and mass transport coefficients of 10−6-10−5m/s it has up limitation.With the help of a TIRF-flow-through shear analyzer in which a certain volume unit of an immiscible fluid, for example an air bubble, is fed into the buffer flow, an ultra-thin liquid layer arises on the surface with a thickness of 100-200 nm, wherein interface surfaces below 10 nm thickness are technically possible.The new TIRF-flow-through shear analyzer therefore allows the generation of ultra-thin liquid layers while increasing the mass transport coefficients for proteins by 50-100-fold so that the sorption rate constants can be determined without transport limitation.

REFERENCES:
patent: 4028056 (1977-06-01), Snyder et al.
patent: 4413505 (1983-11-01), Matson
patent: 5972710 (1999-10-01), Weigl et al.
patent: 6184978 (2001-02-01), Kasdan et al.

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