Organic compounds -- part of the class 532-570 series – Organic compounds – Amino nitrogen containing
Patent
1980-01-25
1982-01-19
Lusignan, Michael R.
Organic compounds -- part of the class 532-570 series
Organic compounds
Amino nitrogen containing
106 1817, 106 1819, 252608, 4273933, 564 15, C07C12700, B05D 302, C09D 516, C09D 518
Patent
active
043118550
ABSTRACT:
An improved process for manufacturing tetrakis (hydroxymethyl) phosphonium amide condensation product without the formation of a precipitate. Urea or thiourea is added to the tetrakis (hydroxymethyl) phosphonium salt having an anion formed from a dibasic or tribasic or polybasic acid. The said salt is in aqueous solution. The pH of the aqueous solution of said salt is adjusted to the range of 4-6.5 when the urea or thiourea is added to the salt. The proportion of said salt to said urea or thiourea is 1:0.05-0.5 (molar). The sulphuric acid salt is preferred. The process produces an improved aqueous product substantially free of insolubles.
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patent: 4110509 (1978-08-01), Roth
Cole Robert
Stephenson James E.
Albright & Wilson Ltd.
Lusignan Michael R.
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