Filtration member for solid-liquid separation

Liquid purification or separation – Filter – Supported – shaped or superimposed formed mediums

Reexamination Certificate

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Details

C210S483000, C210S500100, C442S040000, C442S041000

Reexamination Certificate

active

06318565

ABSTRACT:

BACKGROUND OF THE INVENTION
The invention relates to a filter medium for solid/liquid separation, preferably as a deposit support for a deposit filter and for cake-forming filtration according to the type specified in the preamble of claim
1
.
The operating principle of deposit filters includes the initial deposition of a filter layer which extends across the openings of a deposit support. First, a base deposition is carried out to form a first pre-deposit by flowing the deposit material in a fast circulation through the filter so that in this manner a thin layer of particles is formed on the filter surfaces. Since the deposit material, in many applications silica gel, has a particle spectrum of 0.3 &mgr;m to approximately 50 &mgr;m, and the deposit support has usually openings of a magnitude of 60 &mgr;m to 100 &mgr;m, the deposit layer can be formed only when a plurality of particles become wedged in the opening so as to form a bridge so that thereby penetration of the opening is hindered. With the second initial deposition a cake of a layer thickness of 0.5 mm to 1.0 mm is then built.
According to the operating principle of a cake-forming filtration, foreign filter aids that are deposited onto a filter medium are completely unnecessary. The solids which are contained in the suspension to be filtered grow directly on the surface of the filter medium to a deposit or filter cake while the filtrate is removed through the filter medium.
Depending on the field of application of the filter different filter media can be used. Deposit supports comprised of a plastic fabric or a metal fabric as well as slotted sieves are the most common embodiments for a deposit filtration. For filters such as single layer filters or suction filters or single layer process filters or dry filters it is also known to employ sinter materials such as, for example, multi-layer sinter fabrics, sinter fleece, or sintered powder sheets. An opening magnitude of approximately 55 &mgr;m is the lower limit of practical, useful structures in the known fabric embodiments because for a mesh width that is smaller the fibers would have to be so thin that the rip stability no longer would be sufficient. Moreover, the ratio of the surface area of the openings to the total surface area is fixed and not variable.
It is an object of the present invention to provide a filter medium for the solid/liquid separation that, even for low particle size or fine particle size distribution of the filter aid, quickly and reliably forms a stable uniform filter layer across the entire filter surface.
SUMMARY OF THE INVENTION
This object is solved by a filter medium with the features of claim
1
.
The essential advantages of the invention are that due to the minimal size of the openings the filter cake is formed much quicker or the required filter layer is deposited faster; in the latter case only a single pre-deposit is required. This results in a considerable reduction of cost due to time savings and reduced amounts of the required filter aid. The inventive filter medium is robust and has a long service life. Furthermore, it can be cleaned easily because of its smooth surface. Back flow properties for the purpose of cleaning are also realized because of the form stability of the material. The filter medium is comprised of a thin plate or foil and can be produced inexpensively as a drawn grid structure that, in comparison to metal fabrics, has substantially improved filtration properties. This is so because the risk that the deposit layer will collapse in the area of one or more openings and thus reduce the filter effect is considerably reduced. Drawn grid structures are known in the art. However, they are conventionally produced with large mesh width, i.e., the proportion of openings relative to the total surface area is large (compare DIN 791).
Since a single pre-deposit is sufficient and a filter aid of medium to fine particle size distribution is sufficient for this purpose, such a filter medium is suitable also for use of regenerated diatomaceous earth and other filter media that can be regenerated as well as different absorption media.
The filter medium comprises a certain form stability that depends, of course, on the thickness of the plate and the type of material, as well as on the number and size of the openings in the plate. Since therefore a large number of parameters must be taken into consideration, shaped parts of a suitable shape can be produced and adapted for the respective use, for example, as a hollow cylinder, as a tub or disk-shaped structure, etc.
Since the individual openings of the plate forming the filter medium are not connected to one another, no transverse flow can occur within the plate so that the edge portion of the filter medium in can be sealed in a simple manner. The plate can be used on all disk filter elements that in the past have been provided with conventional fabrics without having to change the fastening device. This not only allows to fit new filter elements directly without system changeover with the inventive filter medium, but it is also possible to retrofit already operating filters without problems.
The inventive filter medium provides the possibility to vary the free opening surface area relative to the total surface area of the filter medium over a large range. This can be achieved by varying the opening size and the number of openings. The opening size can be determined by the manufacturing tool. A special advantage is that with the invention a free opening surface area can be achieved which is, for example, in the range of 0.5% to 15.0% of the total surface area of the filter medium. The height distribution of the filter cake can thus be more uniform. This effect is especially extremely important in the first phase of the filtration. A further possibility of affecting the opening size is their size determination via the amount of the reverse deformation so that the respectively set requirements with respect to the free opening surface area and the opening size can be taken into consideration.
The material thickness of the thin plate or of the foil, is preferably 0.1 mm to 1.5 mm. The material thickness can be determined as a function of the mechanical properties of the respective material and the required stiffness of the filter medium. The material for the filter medium is especially stainless steel or stainless steel alloys, non-iron metals or aluminum alloys or other corrosion-resistant materials, especially plastic. The selection should be based on the respective mechanical and/or chemical requirements.
The smooth surface area of the plate provides very good cake removal for horizontal disk filters which are rotated for this purpose so that the filter cake is spun off in the outward direction. Furthermore, the material has no preferred orientation, which is especially important when employing the material on rotating filter elements with radial symmetry stress. Depending on the respective metal, welding of the filter medium is possible which may be advantageous when a filter medium is comprised of a plurality of parts or is to be connected to supporting elements.
The invention allows the production of slot widths up to a minimum of approximately 5 &mgr;m. Depending upon the employed filter aids and the consistency of the liquid to be filtered, slot widths between 5 &mgr;m and 300 &mgr;m can be viewed as the preferred slot width. The length of the slots is preferably between 0.5 mm and 15 mm.
The reverse deformation of the drawn grid structure is preferably carried out by rolling so that the desired final dimensions are very precisely achieved. In this manner, a high finishing precision with a uniform and constant product quality results. The openings extend in the filter medium substantially at a right angle to the surface of the filter medium so that the openings can be cleaned easily because the openings open slightly conically and are clearly defined. The surface of the filter medium can be electrochemically treated for producing special surface properties or can be mechanica

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