Filtration adjuvants, filtration supports, filtration process us

Food or edible material: processes – compositions – and products – Fermentation processes

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Details

426 7, 426 12, 435220, 435221, 210777, 210778, 210741, 210193, 210792, 210797, 210269, C12C 1100, C12C 700, C12C 728

Patent

active

061174599

DESCRIPTION:

BRIEF SUMMARY
BACKGROUND OF THE INVENTION

The present invention concerns new filtration adjuvants, usable in the filtration of liquids, particularly beer at the end of the secondary fermentation storage. It also concerns a new filtration method using said new filtration adjuvants. It finally concerns a new method of regeneration in situ of said filtration adjuvants and new filtration supports.
Filtration adjuvants are substances used in solid-liquid separation in which a deposit is formed on a filter screen or a filter support, either alone or mixed with the substances to be retained, and procure efficient separation by primarily mechanical means.
The various types of filtration adjuvant can be distinguished by their main ingredients.
The type of filtration adjuvant most frequently used in brewing is kieselguhr, comprising mainly calcined diatoms.
Other types of filtration adjuvants include perlite obtained from volcanic rock, starch, cellulose and fibrous polymer synthetic materials.
During filtration, these various filtration adjuvants form a porous medium trapping the impurities to be eliminated and facilitating the flow of the liquid phase.
The filtration adjuvants described above can be used either in the so-called pre-layer technique or in the so-called "alluvion" technique.
One industrial sector in which filtration adjuvants are used is brewing.
Most commercially produced beers must have a bright color and be free of micro-organisms. These requirements are generally complied with when the beer has an E.B.C. (European Brewing Convention) clarity value less than 0.5.degree. EBC and a micro-organism content less than five yeasts per liter.
The E.B.C. clarity values and their assessment are defined in the publication: Analytica-E.B.C., 4th Ed., 1987, Revue de la Brasserie et des Boissons Ed., Zurich.
Until now the most economic and efficient method of obtaining these values has been to use a filtration adjuvant in making the beer.
After it has matured in secondary fermentation storage tanks, the beer must be clarified and filtered before it is packaged in order to eliminate a number of impurities, including colloidal material that makes it cloudy and yeast. After filtration the beer has a bright color and sufficient stability for an adequate shelf life.
Beer is usually filtered using filtration adjuvants and one of the following two techniques, namely "mass" filtration or "alluvion" filtration, the latter requiring a preliminary layer to be formed beforehand.
"Alluvion" filtration, by far and away the more commonly used technique, consists in depositing onto the filter medium, prior to filtration proper, a first preliminary layer of coarse filtration adjuvant to protect the filtration support (for example multiple tube filters or plate filters) and to facilitate demounting of the filter after filtration and cleaning of the filtration support. A second preliminary layer of filtration adjuvant similar in size to that used for "alluvion" filtering is frequently deposited in order to obtain a clear filtrate as soon as the filtration cycle starts.
In "alluvion" filtration, the filtration adjuvant is mixed with the beer before it is filtered and forms a suspension. During filtration this suspension forms a mixed cake containing impurities and the filtration adjuvant.
When the filtration cycle is finished, the filtration adjuvant cake containing the trapped impurities, in particular the yeasts, is eliminated in the form of a thick suspension generally referred to as slurry ("bourbe").
When multiple tube filters are used to carry out the filtration, a counterflow of a pressurized gas-water emulsion through the filter medium detaches the cake from the filter medium. It drops to the bottom of the filtration tank, where it is recovered.
If horizontal plate filters are used to carry out the filtration, the cake is eliminated by the centrifugal force produced by rotating the filter plates.
In "mass" filtration, the filtration adjuvant is deposited directly onto the filter support before the beer is filtered.
Using filtration adj

REFERENCES:
patent: 3220928 (1965-11-01), Brenner
patent: 3550774 (1970-12-01), Hirs et al.
patent: 4028255 (1977-06-01), Bolto et al.
patent: 4350620 (1982-09-01), Hartinger et al.
patent: 4820420 (1989-04-01), Hums et al.
patent: 5801051 (1998-09-01), Kiefer et al.
Hardwick, William A., Handbook of Brewing, p. 325-326, 1995.
Varnum, Alan, H. and Jane P. Sutherland, Beverages--Technology, Chemistry and Microbiology, p. 324-325, 1994.
Boschet, Gianmario, Stabilization of Beer With the Use of PVPP and Silicon Gel Products, Bios, vol. 17, No. 8-9, pp. 49-52 (Translation), Aug. 1986.
Schafft, H., N. Mums and G. Muller, PVPP Recycling For Beer Stabilization, Brauwelt, p. 1376-1378, 1380-1382 (Translation), Sep. 1977.
Donhauser, S., D. Wagner and C. Waubke, Beer Filtration Without Kieselguhr, Brauwelt, vol. 42, p. 1838-1841, 1844, 1846 (Translation), 1988.
Abstract of Czech Patent No. 227470, vol. 105, No. 17, Oct. 27, 1986, "Pulverised Polyamide Sorbent Based on Lignin", By Kralicek et al., p. 567.
Abstract of Russian Patent No. 270739, vol. 73, No. 19, Nov. 9, 1970, "Lactams", By Moskovich, p. 331.
Japanese Patent Abstract No. 3169311, vol. 15, No. 409 (C-0876), Oct. 18, 1991, "Multilayer Filter Cartridge", By Teisho.

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