Falling film aluminoxane process

Organic compounds -- part of the class 532-570 series – Organic compounds – Aluminum containing

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C07F 506

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active

049373633

ABSTRACT:
Alkylaluminoxanes are made by conducting a solution of an alkylaluminum (e.g. trimethyl aluminum) in an inert solvent to the top of an upright hollow column and allowing the solution to flow as a thin film down the inner surface of the column while passing a wet inert gas (e.g. nitrogen) up through the column such that the wet inert gas contacts the thin falling film of alkyl aluminum solution forming alkylaluminoxane.

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patent: 4665208 (1987-05-01), Welborn, Jr. et al.
patent: 4730071 (1988-03-01), Schoenthal et al.
patent: 4730072 (1988-03-01), Schoenthal et al.

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