Fabricating crosslinked polyimide high temperature composites an

Stock material or miscellaneous articles – Composite – Of polyimide

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1563074, 1563311, 427 38, 528339, 528347, B32B 2700

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active

051789647

ABSTRACT:
A polyimide resin or composite may be pretreated by heating a reaction mixture that initially includes an aromatic diamine monomer, an end cap monomer, and an aromatic dianhydride monomer to a temperature between about 250.degree. C. and about 300.degree. C. for a period sufficient to completely imidize the reaction mixture to an imide resin without substantial crosslinking. A crosslinked reinforced polyimide composite article may be fabricated by heating a plurality of prepregs to a first temperature between about 250.degree. C. and about 300.degree. C. for a first period sufficient to completely imidize the prepreg without substantial crosslinking. Each prepreg has a plurality of reinforcing fibers and a reaction mixture. The prepregs are stacked in a desired orientation to form a laminated structure before or after heating to the first temperature and further heated at a superatmospheric pressure to a second temperature for a second period to form a crosslinked reinforced polyimide composite article by consolidating the prepregs and crosslinking the imide resin in the prepreg.

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"Processing of PMR-15 Prepregs for High Temperature Composites," by Mel Kantz, published in Plastics Engineering, vol. 46, No. 1, Jan. 1990, at pp. 27-30.

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