Liquid purification or separation – Processes – Liquid/liquid solvent or colloidal extraction or diffusing...
Patent
1994-07-13
1997-05-13
Spear, Frank
Liquid purification or separation
Processes
Liquid/liquid solvent or colloidal extraction or diffusing...
210259, B01D 1104
Patent
active
056289065
ABSTRACT:
The invention relates to an extraction process which comprises adding a primary solvent to a first solution containing a solute dissolved in a native solvent. The primary solvent is added in an amount sufficient to form a single-phase mixture comprising said primary solvent, said native solvent and said solute. Thereafter a modifier is added to the single-phase solution. The modifier is miscible with either the primary solvent or the native solvent and serves to reduce the miscibility of the primary solvent with the native solvent so as to form a two-phase mixture. The two phases are allowed to separate into one phase rich in the native solvent and a second phase rich in the primary solvent and solute. Finally, the solute is separated from the solvent-rich phase. The process is particularly useful for separating products of fermentation from fermentation broths or other systems which are sensitive to high temperatures or which tend to form emulsions.
REFERENCES:
patent: 2250976 (1941-07-01), Van Dijck
patent: 2361780 (1944-10-01), Lewis
patent: 3427357 (1969-02-01), de Gramont et al.
patent: 3898291 (1975-08-01), Darsi et al.
patent: 3936489 (1976-02-01), Rozsa et al.
patent: 4261818 (1981-04-01), Sweeney
patent: 4336106 (1982-06-01), Winter, III
patent: 4493765 (1985-01-01), Long et al.
patent: 4632809 (1986-12-01), Otto et al.
patent: 4732685 (1988-03-01), Brandt et al.
patent: 4770780 (1988-09-01), Moses
patent: 4863607 (1989-09-01), Andrew et al.
patent: 4877530 (1989-10-01), Moses
patent: 4954260 (1990-09-01), Ludmer et al.
patent: 5049279 (1991-09-01), Bitar et al.
patent: 5078886 (1992-01-01), Hsu
patent: 5244575 (1993-09-01), Marshall
patent: 5282974 (1994-02-01), Hart
P. A. Schweitzer, ed., Handbook of Separation Techniques for Chemical Engineers, New York: McGraw Hill, selected pages.
R. Blumberg, Liquid-Liquid Extraction, London: Academic Press (1988), pp. 43-44, 52-54.
Z. Ludmer et al., "Solubility in Binary Mixtures at the Immiscibility Critical Point," AIChE Journal, 33:11 (Nov. 1987), pp. 1776-1780.
A. Ullmann et al., "Novel Separation Process Using Solvents with a Critical Point of Miscibility," Proc. A.I.Ch.E. Conference, Miami, Florida (1993).
A. Veide et al., "A Process for Large-Scale Isolation of .beta.-Galactosidase from E. Coli in an Aqueous Two-Phase System," Biotechnolgy and Bioengineering, vol. XXV (1983), pp. 1789-1800.
T. P. Castor et al., "Determination of Taxol in Taxus Media Needles in the Presence of Interfering Components," Journal of Liquid Chromatography, 16(3), 723-731 (1993).
Matkovich et al. Salting-out Acetone from Water-Basis of a New Solvent Extraction System, from Anal. Chem., vol. 45, No. 11, 9-1973, pp. 1915-1921.
Mauri Roberto
Shinnar Reuel
Spear Frank
The Research Foundation of the City University of New York
LandOfFree
Extraction process does not yet have a rating. At this time, there are no reviews or comments for this patent.
If you have personal experience with Extraction process, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Extraction process will most certainly appreciate the feedback.
Profile ID: LFUS-PAI-O-1382481