Explosion proof microwave heated solvent extraction apparatus

Chemical apparatus and process disinfecting – deodorizing – preser – Analyzer – structured indicator – or manipulative laboratory... – Means for analyzing gas sample

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422107, 422109, 422113, 422117, 219679, 219716, G05D 1608, H05B 680

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054437954

ABSTRACT:
An explosion proof microwave heated solvent extraction apparatus or system for extracting organic materials includes a pressure resistant microwave transmissive extraction container, which is preferably of reinforced polyetherimide lined with fluoropolymer, in a microwave radiation heated chamber, with a device for controlling a microwave radiation generator, such as a magnetron, in response to the presence of any solvent vapor in a collection container for rupture diaphragm discharged material from an extraction container or in exhaust gas from the chamber. The presence of the solvent in the collection container or exhaust gas is preferably detected by a semiconductor gas sensor which decreases its electrical resistance in the presence of solvent vapors, thereby increasing its voltage and thus controlling operation of the magnetron, turning it off when solvent vapor (and a potentially explosive gas mixture) is present. Also described are other explosion prevention systems, including a fluoropolymer sheet covering a chamber ceiling and ceiling light, and a process for safely extracting organic materials, utilizing the described apparatus.

REFERENCES:
patent: 4311895 (1982-01-01), Tanabe
patent: 4347216 (1982-08-01), Kawasaki et al.
patent: 4637145 (1987-01-01), Sugisawa e tal.
patent: 4877624 (1988-04-01), Floyd et al.
patent: 5230865 (1993-07-01), Hargett et al.
Figaro Gas Sensor TGS 822, Jan. 1989, 8 Pages.
Figaro Product Information, TGS-822, Aug. 1992, 2 Pages.
Figaro Products Catalog, Sep. 1992, 12 Pages.

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