Ester resolution process

Details Ester resolution process Ester resolution process

1979-09-24

1981-03-03

Trousof, Natalie

Organic compounds -- part of the class 532-570 series

Organic compounds

Carboxylic acid esters

560 35, 560 38, C07C 6972

Patent

active

042542790

ABSTRACT:
Optically active 1-Trichloromethyl-3-methyl-2-butenyl acetoacetate is prepared by resolving the racemic ester via a crystalline enamine derivative.

REFERENCES:
patent: 2577900 (1951-12-01), Lisk et al.
patent: 4024163 (1977-05-01), Elliott et al.
patent: 4027037 (1977-05-01), Siegle et al.
Adams et al., J.A.C.S., 88, 162, 1966.
Potapor et al., Chem. Absts., 3352(g) vol. 57, 1962.
Coward et al., J.A.C.S., 91, 5329, 1969.
G. Stork et al., J.A.C.S., 85, 207 (1963).

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