Electron spin resonance spectrometer

Electricity: measuring and testing – Particle precession resonance – Using an electron resonance spectrometer system

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324300, G01R 3320

Patent

active

048036242

ABSTRACT:
An electron spin resonance spectrometer is disclosed which includes a sample and a reference arm (16, 18). The sample arm has a circulator (30) for directing radiation to a resonator (22) in which a sample for analysis is deposited and for receiving radiation from the resonator and directing it to a detector (32). The detector detects the microwave radiation from the sample and reference arms (16, 18) to determine a property or properties of said sample. The sample arm (16) and said reference arm (18) are formed as an integrated microwave bridge which includes a divider (14) having a first output portion coupled to an attenuator (20), said attenuator being coupled to said circulator (30) by a microwave transmission line (110). The circulator (30) is coupled to at least one output by a second microwave transmission line (124). The divider (14) has a second output portion coupled to a phase shifter (36), said phase shifter including a second circulator (73) and a second attenuator (38) including a third circulator (81), said second circulator (73) being coupled to said third circulator (81) by a third microwave transmission linne (80), a fourth microwave transmission line (90) coupling an output of said third circulator (81) to at least one second output.

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Kangelberg et al., "MIC-Mischer fur Homodyn-Mikrowellenstrecken in EPR-Spektrometern" (MIC Mixers for Homodyne Microwave Routes in EPR Spectrometers), Eletronik, vol. 31, pp. 148-153, 1981.
Denisov, "A Block for Electronic Digital Sweep of a Magnetic Field for Microwave Electron Paramagnetic Resonance Spectrometers," Instruments and Experimental Techniques, vol. 19(1), Part 2, Jan.-Feb., 1976, pp. 291-293.

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