Electrolytic reduction of aromatic steroids

Details Electrolytic reduction of aromatic steroids Electrolytic reduction of aromatic steroids

1976-06-08

1977-09-27

Edmundson, F.C.

Chemistry: electrical and wave energy

Processes and products

C25B 304

Patent

active

040509982

ABSTRACT:
.DELTA..sup.1,3,5(10) STEROIDS ARE ELECTROCHEMICALLY REDUCED TO .DELTA..sup.2,5(10) STEROIDS IN AN IMPROVED MANNER BY CONDUCTING THE REDUCTION IN LIQUID AMMONIA IN THE PRESENCE OF AN ELECTROLYTIC SALT CONSISTING OF AN ALKALI METAL SALT OF A STRONG ACID, WHEN THE ELECTROLYSIS IS CONDUCTED IN A DIVIDED CELL, AND CONSISTING OF AN ALKALI METAL SALT OF A WEAK ACID OR A MIXTURE OF AN ALKALI METAL SALT OF A WEAK ACID AND OF A STRONG ACID, WHEN THE ELECTROLYSIS IS CONDUCTED IN AN UNDIVIDED CELL.

REFERENCES:
patent: 3444057 (1969-05-01), Throop
patent: 3469008 (1969-09-01), Schmidt
patent: 3492207 (1970-01-01), Yang et al.
patent: 3720694 (1973-03-01), Junghans et al.

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