Electrolytic preparation of orthoalkyl-2-halo-N-acylanilides

Details Electrolytic preparation of orthoalkyl-2-halo-N-acylanilides Electrolytic preparation of orthoalkyl-2-halo-N-acylanilides

1983-09-07

1985-01-15

Niebling, John F.

Chemistry: electrical and wave energy

Processes and products

204 59R, 204 72, C25B 300

Patent

active

044937555

ABSTRACT:
orthoAlkyl-orthotrifluoromethyl-2-chloroacetanilides and related compounds are prepared by electrolytic reduction with sulfide cleavage of benzylsulfonium salts with requisite chloroacetylamino and trifluoromethyl substituents on the benzyl group. The compounds are useful as intermediates for conversion to herbicidal compounds.

REFERENCES:
patent: 3480525 (1969-11-01), Wessling et al.
patent: 3480527 (1969-11-01), Wessling et al.
patent: 3616314 (1971-10-01), Settineri et al.
patent: 3660257 (1972-05-01), Settineri et al.
patent: 4172095 (1979-10-01), Steinman et al.
patent: 4209464 (1980-06-01), Steinman et al.
patent: 4404069 (1983-09-01), Goodin et al.
Shono et al, Tetrahedron Letters, vol. 29, pp. 817-821.
The Chemistry of the Sulphonium Group, (copyright 1981, John Wiley; edited by C. J. M. Sterling et al), Chapter 7, Electrochemistry of the Sulphonium Group, J. Grinshaw, pp. 141-155.
Chambers et al., J. Electronal. Chem., vol. 87, (1978), pp. 235-250.

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