Electrochemical synthesis of diaryliodonium salts

Chemistry: electrical and wave energy – Processes and products

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C25B 300

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052777677

ABSTRACT:
Electrochemical process for preparing diaryliodonium salts using a single compartment and a carbon anode. The process has high current efficiency and, optionally, increased para, para' regioselectivity. The process proceeds in the presence of a solvent such as acetic acid and an electrolyte such as a compound of fluorine or sulfuric acid.

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