Dynamically balanced, differential gas adsorption appartaus

Measuring and testing – Particle size

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G01N 1508

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active

051332191

ABSTRACT:
An apparatus and method are disclosed for obtaining adsorption data to be used for surface area and pore volume analysis. The apparatus and method utilize the differential pressures between a pair of dosing systems to indicate the amount of gas adsorbed by a sample. The system doses a sample chamber and a null chamber from essentially equal volumes of gas, and causes the chambers to be dosed such that any pressure difference between them, caused by adsorption, is eliminated. The resulting differential pressure between the essentially equal volumes of gas then indicates the amount of gas adsorbed by the sample. The system may be operated to dose in equilibrated increments or in a scanning mode in which adsorbate gas is continuously leaked into the sample chamber. A feedback circuit then controls dosing into the null chamber to eliminate the pressure difference caused by adsorption onto the sample surface. A differential pressure transducer connecting the volumes from which the gas is released then indicates the amount of gas adsorbed.

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