Dynamic background signal exclusion in chromatography/mass...

Radiant energy – Ionic separation or analysis

Reexamination Certificate

Rate now

  [ 0.00 ] – not rated yet Voters 0   Comments 0

Details

C250S282000, C250S288000

Reexamination Certificate

active

07009174

ABSTRACT:
A method and system for obtaining mass spectrographic data of a substance. The method includes (a) subjecting the substance to a chromatographic process and ionizing the output thereof; (b) obtaining a current mass spectrogram of the output; (c) identifying at least one ion having a fast rising mass signal by comparing the current mass spectrum obtained In step (b) against one or more previously acquired mass spectrums of the output; and (d) fragmenting the identified ion and recording a mass spectrum resulting therefrom. A mass spectrometer system, includes a chromatography column; a mass spectrometer, including an ion source for ionizing the output of the chromatographic column, in which the mass spectrometer is capable of isolating, fragmenting and mass analyzing an ion of selected mass; and a data-dependent, data acquisition controller programmed to operate the mass spectrometer so as to obtain a current mass spectrogram of the output, identify one or more ions having fast rising mass signals by comparing the current mass spectrum against one or more previously acquired mass spectra of the output, and fragmenting of said identified ions and recording a mass spectrum resulting therefrom.

REFERENCES:
patent: 2002/0009394 (2002-01-01), Koster et al.
patent: 2004/0181351 (2004-09-01), Thompson et al.
patent: 2005/0001163 (2005-01-01), Belov et al.
Covey, T.R. et al., “High-Speed Liquid Chromatography/Tandem Mass Spectrometry for the Determination of Drugs in Biological Samples”, Anal. Chem, 58(12):2453-2460, Oct. 1986.
Yu, X et al., “A Novel LC/MS Background Subtraction Technique for the Detection of Drug Metabolites in Biological Samples . . . ” Merck Research Labs., West Point, PA 19486.
Windig, W. et al., “A Noise and Background Reduction Method for Component Detection in Liquid Chromatography/Mass Spectrometry”, Anal. Chem., 68(20):3602-3606, Oct. 1996.

LandOfFree

Say what you really think

Search LandOfFree.com for the USA inventors and patents. Rate them and share your experience with other people.

Rating

Dynamic background signal exclusion in chromatography/mass... does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Dynamic background signal exclusion in chromatography/mass..., we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Dynamic background signal exclusion in chromatography/mass... will most certainly appreciate the feedback.

Rate now

     

Profile ID: LFUS-PAI-O-3539968

  Search
All data on this website is collected from public sources. Our data reflects the most accurate information available at the time of publication.