Dual x-ray fluorescence spectrometer and method for fluid...

X-ray or gamma ray systems or devices – Specific application – Fluorescence

Reexamination Certificate

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C378S044000, C378S045000

Reexamination Certificate

active

06859517

ABSTRACT:
Disclosed are an X-ray fluorescence (SRF) spectrometer and method for on-site and in-line determination of contaminant elements in lubricating oils and in fuel oils on board a marine vessel. An XRF source block13contains two radionuclide sources16, 17(e.g. Cd109and Fe55), each oriented180degrees from the other to excite separate targets. The Cd109source16excites sample lube oil flowing through a low molecular weight sample line18. The Fe55source17excites fuel oil manually presented to the source beam inside a low molecular weight vial26or other container. Two separate detectors A and B are arranged to detect the fluorescent x-rays from the targets, photons from the analyte atoms in the lube oil for example, and sulfur identifying x-rays from bunker fuel oil for example. The system allows both automated in-line and manual on-site analysis using one set of signal processing and multi-channel analyzer electronics34, 37as well as one computer39and user interface43.

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