Dry process for producing diborane

Details Dry process for producing diborane Dry process for producing diborane

1981-09-18

1983-06-14

Vertiz, O. R.

Chemistry of inorganic compounds

Boron or compound thereof

Binary compound

C01B 610

Patent

active

043882846

ABSTRACT:
Diborane is produced by reacting lithium or sodium borohydride with boron trifluoride in the absence of a solvent, thereby avoiding the dangers associated with the ether solvents previously used in similar reactions. The reaction appears to proceed via hydride abstraction from the borohydride, rather than via the hydride-halide exchange mechanism in the corresponding reaction in ether solution. Yields of about 95% can be achieved.

REFERENCES:
patent: 2543511 (1951-02-01), Sehlesinger
patent: 2888327 (1959-05-01), Adams

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