Disulfonate process control

Chemistry of inorganic compounds – Nitrogen or compound thereof – Oxygen containing

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C01B 21093

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active

050154559

ABSTRACT:
In a process for the production of hydroxylamine disulfonate diammonium salt (DS) comprising feeding an aqueous ammoniuum nitrite solution, SO.sub.2 gas and trim ammonia to a packed column to create a reaction mixture to produce DS; the improvement comprising controlling said process by measuring the pH of the DS product solution stream, comparing said pH with a pre-selected pH value, and adjusting for deviation of pH by adjusting the feed of nitrite solution and measuring the concentration of unreacted nitrite in the DS product solution stream, comparing said concentration with a pre-selected concentration value, and adjusting for deviation of said concentration by adjusting the feed of trim ammonia.

REFERENCES:
patent: 2772145 (1953-02-01), Joris et al.
Patent Abstracts of Japan-vol. 6, No. 131 (C-114) (1009) Jul. 17, 1982; and JP-A-5756308 (Ube Kosan K.K.) 03.04.1982.

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