Distillation method and apparatus for reprocessing sulfuric acid

Distillation: processes – separatory – With disparate physical separation – Of entrained particles from a vapor or gas

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203 12, 203 77, 203 80, 203 86, 203DIG2, 203DIG9, 134 12, 156642, 159 473, 159DIG15, 159DIG19, 202154, 202159, 2021856, 202197, 202205, 2022671, 423531, B01D 310, C01B 1790

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active

049800329

ABSTRACT:
An apparatus and method for reprocessing waste piranha containing contaminated H.sub.2 SO.sub.4 from, for example, a semiconductor processing operation is described. The apparatus and method include a first distillation flask which are maintained under a substantial vacuum. The first distillation flask includes a first column with a column packing means and a reflux means to retard loss of H.sub.2 SO.sub.4 in the first distillation. The second distillation flask boils off substantially pure H.sub.2 SO.sub.4 through a column which is coupled to a condenser which condenses substantially pure H.sub.2 SO.sub.4.

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