Dinitrosyldihalo complexes of molybdenum or tungsten

Details Dinitrosyldihalo complexes of molybdenum or tungsten Dinitrosyldihalo complexes of molybdenum or tungsten

1976-08-18

1978-04-25

Sneed, Helen M. S.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260270PY, 260429R, 260441, 260446, C07D 3124, C07F 1100

Patent

active

040862291

ABSTRACT:
Dinitrosyldihalo complexes of molybdenum or tungsten are produced from (1) an oxytetrahalide of molybdenum or of tungsten, (2) an alkali metal nitrite, (3) a reducing agent which is metallic iron or a borohydride of sodium, potassium, rubidium, or cesium, (4) a ligand-forming compound, (5) in an aprotic diluent.

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patent: 3691144 (1972-09-01), Zuech
patent: 4012399 (1977-03-01), Hechenbleikner et al.
Feltham, Inorganic Chemistry, v1, pp. 116-119, (1964).
Bencze, J. Organometallic Chemistry, v56, pp. 303-306, (1973).
Cotton et al., Inorganic Chemistry, v3, pp. 1609-1612, (1964).
Bencze et al., J. Organometallic Chem., v70, pp. 421-425, (1974).
Hughes et al., Inorganic Chem., v12, pp. 471-473, (1973).
McCleverty et al., J. Chem. Soc. Dalton Trans., pp. 2588-2593, (1972).
Hughes, Advances in Chemistry Series, No. 132, pp. 192-211, (1974).

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