Digestion apparatus useful for a kjeldahl method

Chemistry: analytical and immunological testing – Including sample preparation – Digestion or removing interfering materials

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422 78, 422 79, 422 80, 422102, 422103, 422104, 219 1055R, 219 1055A, 219 1055D, 2504551, 34 1, G01N 100

Patent

active

048822868

ABSTRACT:
A microwave-based apparatus for rapid digestion of a sampel by a Kjeldahl method is provided which includes a reaction vessel surrounded by an insulator in the form of, for example, a cup. The reaction vessel is disposed in the internal chamber of a microwave system, which includes a wall having an aperture. A connector tube is slidably disposed in the aperture, wherein one end of the tube is connected to the mouth of the reaction vessel, and the other end is connected to a suction device external to the chamber. A biasing element is provided outside the chamber to assist in joining the slidable connector tube to the mouth of the vessel, yet enabling removal of the vessel from the chamber without detachment of the biasing element.

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P. Barrett et al, Analytical Chemistry, 7, 1021 (1978), Prolabo Literature.
Bradstreet, The Kjeldahl Method for Organic Nitrogen, 1965, pp. 40-42.
Kjel-Foss Automatic Literature by A/S N. Foss Electric.
S. Brayton of the Hach Company, "A Practical Kjeldahl-Nitrogen Method".

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